2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

Base Information

Chemical Name:2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate
CAS No.:1552301-93-5
Molecular Formula:C₂₀H₂₀O₇
Molecular Weight:372.375
Hs Code.:

Synonyms:2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

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Chemical Property of 2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

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Technology Process of 2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

There total 4 articles about 2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 953422-33-8
2-(4'-hydroxyphenyl)ethyl methyl carbonate

: 144256-14-4
(E)-methyl 3-(4-acetoxy-3-methoxyphenyl)acrylate

: 1552301-93-5
2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

Guidance literature:: With trifluoroacetic acid; for 6h; Temperature; Reflux;
DOI:10.1039/c3nj01180a

Reference yield:

: 2596-47-6,147677-05-2,34749-55-8
(E)-3-(4-acetoxy-3-methoxyphenyl)acrylic acid

: 1552301-93-5
2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 8 h / 25 °C

2: trifluoroacetic acid / 6 h / Reflux

With potassium carbonate; trifluoroacetic acid; In acetone;
DOI:10.1039/c3nj01180a

Reference yield:

: 1135-24-6,537-98-4
3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 1552301-93-5
2-[4-(4-hydroxy-3-methoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 24 h / 25 °C

2: potassium carbonate / acetone / 8 h / 25 °C

3: trifluoroacetic acid / 6 h / Reflux

With pyridine; potassium carbonate; trifluoroacetic acid; In acetone;
DOI:10.1039/c3nj01180a