dimethyl (2S,3S)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate

Base Information

• Chemical Name: dimethyl (2S,3S)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate
• CAS No.: 1620320-06-0
• Molecular Formula: C₄₂H₅₂O₆Si₂
• Molecular Weight: 709.042

Synonyms:dimethyl (2S,3S)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate

Chemical Property of dimethyl (2S,3S)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate

Chemical Property:

Purity/Quality:

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Technology Process of dimethyl (2S,3S)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate

There total 1 articles about dimethyl (2S,3S)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon monoxide (201230-82-2) + 1,2-bis((tert-butyldiphenylsilyloxy)methyl)-3-methylenecyclopropane → dimethyl (2R,3R)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate (1620320-07-1) + dimethyl (2S,3S)-2,3-bis((tert-butyldiphenylsilyloxy)methyl)-4-methylenepentanedioate (1620320-06-0)

Guidance literature:

With copper(I) triflate benzene complex; (4S,4'S)-4,4'-bis(naphthalen-1-ylmethyl)-4,4',5,5'-tetrahydro-2,2'-bioxazole; oxygen; palladium dichloride; In tetrahydrofuran; methanol; at 20 ℃; for 30h; Overall yield = 82 %; Overall yield = 289mg; Inert atmosphere;

DOI:10.1016/j.tetasy.2014.05.007

upstream raw materials:

carbon monoxide

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