Technology Process of Dimethyl 4,4'-<(3-Benzyloxy-1,1-propanediyl)bis(oxy)bis(1,2-ethanediyl)>bisbenzoate
There total 4 articles about Dimethyl 4,4'-<(3-Benzyloxy-1,1-propanediyl)bis(oxy)bis(1,2-ethanediyl)>bisbenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at -70 ℃;
for 96h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) BH3*S(CH3)2, 2.) H2O2 (30percent) / 1.) THF, 2 h, room temperature, 2.) 1 h, room temperature
2: 93 percent / hexamethyldisilazane, pyridine / 3 h / Ambient temperature
3: 73 percent / TMS triflate / CH2Cl2 / 96 h / -70 °C
With
pyridine; dimethylsulfide borane complex; dihydrogen peroxide; 1,1,1,3,3,3-hexamethyl-disilazane;
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / SOCl2
2: 1.) BH3*S(CH3)2, 2.) H2O2 (30percent) / 1.) THF, 2 h, room temperature, 2.) 1 h, room temperature
3: 93 percent / hexamethyldisilazane, pyridine / 3 h / Ambient temperature
4: 73 percent / TMS triflate / CH2Cl2 / 96 h / -70 °C
With
pyridine; thionyl chloride; dimethylsulfide borane complex; dihydrogen peroxide; 1,1,1,3,3,3-hexamethyl-disilazane;
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
