C₁₁H₁₁⁽²⁾H₃

Base Information

Chemical Name:C₁₁H₁₁⁽²⁾H₃
CAS No.:89437-72-9
Molecular Formula:C₁₁H₁₄
Molecular Weight:149.208
Hs Code.:

C<sub>11</sub>H<sub>11</sub><sup>(2)</sup>H<sub>3</sub>

Synonyms:C₁₁H₁₁⁽²⁾H₃

Suppliers and Price of C₁₁H₁₁⁽²⁾H₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₁⁽²⁾H₃

Chemical Property:

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Technology Process of C₁₁H₁₁⁽²⁾H₃

There total 5 articles about C₁₁H₁₁⁽²⁾H₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34713-70-7
2-Phenylpropanal

: 89437-72-9
C₁₁H₁₁⁽²⁾H₃

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / 1.) NaH / tetrahydrofuran / 2 h / Heating

2: 83 percent / BF₃*Et₂O, AcOH / CHCl₃ / Heating

3: 72 percent / nBuLi, D₂O / hexane; diethyl ether

4: 65 percent / Ce(NH₄)2(NO₃)6 / acetonitrile; H₂O / 0.08 h / 0 °C

5: nBuLi / hexane; diethyl ether / 1.) RT, 4 h; 2.) reflux, 12 h

With n-butyllithium; ammonium cerium(IV) nitrate; boron trifluoride diethyl etherate; water-d2; sodium hydride; acetic acid; In tetrahydrofuran; diethyl ether; hexane; chloroform; water; acetonitrile;
DOI:10.1021/ja00322a042

Reference yield:

: 3805-10-5
2,2-(dimethyl)-2-phenylacetaldehyde

: 89437-72-9
C₁₁H₁₁⁽²⁾H₃

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / BF₃*Et₂O, AcOH / CHCl₃ / Heating

2: 72 percent / nBuLi, D₂O / hexane; diethyl ether

3: 65 percent / Ce(NH₄)2(NO₃)6 / acetonitrile; H₂O / 0.08 h / 0 °C

4: nBuLi / hexane; diethyl ether / 1.) RT, 4 h; 2.) reflux, 12 h

With n-butyllithium; ammonium cerium(IV) nitrate; boron trifluoride diethyl etherate; water-d2; acetic acid; In diethyl ether; hexane; chloroform; water; acetonitrile;
DOI:10.1021/ja00322a042

Reference yield:

: 89278-54-6
2-(1-methyl-1-phenylethyl)-1,3-dithiane

: 89437-72-9
C₁₁H₁₁⁽²⁾H₃

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / nBuLi, D₂O / hexane; diethyl ether

2: 65 percent / Ce(NH₄)2(NO₃)6 / acetonitrile; H₂O / 0.08 h / 0 °C

3: nBuLi / hexane; diethyl ether / 1.) RT, 4 h; 2.) reflux, 12 h

With n-butyllithium; ammonium cerium(IV) nitrate; water-d2; In diethyl ether; hexane; water; acetonitrile;
DOI:10.1021/ja00322a042