[RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)

Base Information

Chemical Name:[RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)
CAS No.:877864-75-0
Molecular Formula:CF₃O₃S*C₃₀H₃₅ClN₃P₂Ru
Molecular Weight:785.169
Hs Code.:

[RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF<sub>3</sub>SO<sub>3</sub>)

Synonyms:[RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)

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Chemical Property of [RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)

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Technology Process of [RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)

There total 2 articles about [RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 877864-66-9
N-methyl-1,3,5-triaza-7-phosphaadamantane trifluoromethanesulfonate

: 877864-75-0
[RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)

Guidance literature:: In acetone; under N2 atm. N-methyl-1,3,5-triaza-7-phosphaadamantane was added to soln. Ru complex in acetone, slowly warmed to reflux and maintained for 4 h; ppt. was filtered while hot, washed with acetone, and vac.-dried; elem. anal.;
DOI:10.1021/ic051053q

Reference yield:

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 877864-66-9
N-methyl-1,3,5-triaza-7-phosphaadamantane trifluoromethanesulfonate

: 877864-75-0
[RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)

: [RuClCp(N-methyl-1,3,5-triaza-7-phosphaadamantane)₂](OSO₂CF₃)₂

Guidance literature:: In acetone; ligand (0.28 mmol) added to acetone soln. of Ru compd. (0.14 mmol), refluxed for 4 h; filtered off, washed (Et2O), dried (vac.);
DOI:10.1016/j.jorganchem.2009.01.050

Reference yield: 92.0%

: 5952-62-5
sodium 4-(diphenylphosphino)benzenesulfonate

: 877864-75-0
[RuCpCl(triphenylphosphine)(N-methyl-1,3,5-triaza-7-phosphaadamantane)](CF₃SO₃)

: cyclopentadienidoruthenium(II)I(PPh₂(3-OSO₂C₆H₄))PPh₃(N-methyl-1,3,5-triaza-7-phosphaadamantane)(CF₃SO₃)

Guidance literature:: In methanol; byproducts: NaCl; (N2), Ru complex and ligand (1:1.17) dissolved in CH3OH, refluxed for 12h; filtered, (glass), evapd.(vac.), washed (Et2O), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200601177