2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester

Base Information

Chemical Name:2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester
CAS No.:1260507-03-6
Molecular Formula:C₂₃H₂₉NO₅
Molecular Weight:399.487
Hs Code.:

Synonyms:2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester

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Chemical Property of 2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester

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Technology Process of 2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester

There total 5 articles about 2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 621-23-8
1,2,3-trimethoxybenzene

: 138350-92-2
tert-butyl 1,2,3,4-tetrahydroisoquinoline-2-carboxylate

: 1260507-03-6
2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester

Guidance literature:: With tert.-butylhydroperoxide; Iron(III) nitrate nonahydrate; In decane; at 0 - 50 ℃;
DOI:10.1039/c0cc02491k

Reference yield: 64.0%

: 621-23-8
1,2,3-trimethoxybenzene

: tert-butyl 1-(tert-butylperoxy)-3,4-dihydroisoquinoline-2(1H)-carboxylate

: 1260507-03-6
2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester

Guidance literature:: With methanesulfonic acid; acetic acid; at 20 ℃; for 0.00833333h;
DOI:10.1002/ejoc.201201527

Reference yield:

: 138350-92-2
tert-butyl 1,2,3,4-tetrahydroisoquinoline-2-carboxylate

: 1260507-03-6
2(1H)-isoquinolinecarboxylic acid-3,4-dihydro-1-(2,4,6-trimethoxyphenyl)-1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: decane / 5 h / 105 °C

2: acetic acid; methanesulfonic acid / 0.01 h / 20 °C

With methanesulfonic acid; acetic acid; In decane;
DOI:10.1002/ejoc.201201527