Technology Process of 2-O-methyllecanoric acid
There total 4 articles about 2-O-methyllecanoric acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydrogencarbonate;
In
N,N-dimethyl-formamide;
for 24h;
Ambient temperature;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / dicyclohexylcabodiimide / toluene; diethyl ether / 12 h
2: 90 percent / hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
3: 82 percent / potassium hydrogen carbonate / dimethylformamide / 24 h / Ambient temperature
With
hydrogen; potassium hydrogencarbonate; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
diethyl ether; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / dicyclohexylcabodiimide / toluene; diethyl ether / 12 h
2: 90 percent / hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
3: 82 percent / potassium hydrogen carbonate / dimethylformamide / 24 h / Ambient temperature
With
hydrogen; potassium hydrogencarbonate; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
diethyl ether; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C98082