3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine

Base Information

Chemical Name:3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine
CAS No.:1145787-79-6
Molecular Formula:C₂₆H₃₆N₁₀O₁₄
Molecular Weight:712.63
Hs Code.:

Synonyms:3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine

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Chemical Property of 3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine

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Technology Process of 3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine

There total 1 articles about 3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1134188-59-2
2',3-diazido-1-N-[(S)-4-azido-2-hydroxy-butanoyl]paromamine

: 108-24-7
acetic anhydride

: 1145787-79-6
3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine

Guidance literature:: With pyridine; at -12 ℃; for 8h;

Reference yield: 76.0%

: 1134188-62-7
5-deoxy-5-azido-2,3-di-O-benzoyl-1-O-tricloroacetymido-D-ribofuranose

: 1145787-79-6
3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine

: 1134188-63-8
5-O-(5-azido-2,3-O-dibenzoyl-5-deoxy-β-D-ribofuranosyl)-3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetyl-butanoyl]paromamine

Guidance literature:: 5-deoxy-5-azido-2,3-di-O-benzoyl-1-O-tricloroacetymido-D-ribofuranose; 3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine; In dichloromethane; acetonitrile; at 20 ℃; for 0.166667h; Molecular sieve;

boron trifluoride diethyl etherate; In dichloromethane; acetonitrile; at -20 - -15 ℃; for 0.5h;

With water; sodium hydrogencarbonate; In dichloromethane; acetonitrile;

Reference yield: 76.0%

: 918800-28-9
5-deoxy-5-azido-2,3-di-O-benzoyl-1-O-trichloroacetimido-D-ribofuranose

: 1145787-79-6
3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetylbutanoyl]paromamine

: 1134188-63-8
5-O-(5-azido-2,3-O-dibenzoyl-5-deoxy-β-D-ribofuranosyl)-3',4',6',6-tetra-O-acetyl-2',3-diazido-1-N-[(S)-4-azido-2-O-acetyl-butanoyl]paromamine

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; acetonitrile; at -15 - 20 ℃; Molecular sieve;
DOI:10.1021/jm801640k