C₃₅H₃₈N₂O₁₂

Base Information

Chemical Name:C₃₅H₃₈N₂O₁₂
CAS No.:1383254-81-6
Molecular Formula:C₃₅H₃₈N₂O₁₂
Molecular Weight:678.693
Hs Code.:

C<sub>35</sub>H<sub>38</sub>N<sub>2</sub>O<sub>12</sub>

Synonyms:C₃₅H₃₈N₂O₁₂

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Chemical Property of C₃₅H₃₈N₂O₁₂

Chemical Property:

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Technology Process of C₃₅H₃₈N₂O₁₂

There total 25 articles about C₃₅H₃₈N₂O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1383117-33-6
C₃₅H₃₈N₂O₁₁

: 1383254-81-6
C₃₅H₃₈N₂O₁₂

Guidance literature:: With periodic acid; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja408034x

Reference yield:

: 187040-03-5
4-methylbenzo[1,3]dioxol-5-ol

: 1383254-81-6
C₃₅H₃₈N₂O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: [bis(acetoxy)iodo]benzene / methanol / 0 °C

2.1: water; N,N-dimethyl-formamide / 27 h / 0 - 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 1.66 h / 20 °C

4.1: dihydrogen peroxide; potassium carbonate / water; dimethyl sulfoxide / 4 h / 20 °C

5.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / formic acid / 5 h / 0 °C

6.1: lithium hydroxide monohydrate; water / ethanol / 5 h / Reflux

7.1: tert.-butylnitrite; boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / -15 - 0 °C / Inert atmosphere

7.2: 1 h / 0 - 20 °C

8.1: quinuclidine hydrochloride; methanesulfonamide; potassium hexacyanoferrate(III); osmium(VIII) oxide / water; tert-butyl alcohol / 39 h / 20 °C

9.1: periodic acid / tetrahydrofuran / 1 h / 0 °C

With osmium(VIII) oxide; tert.-butylnitrite; lithium hydroxide monohydrate; methanesulfonamide; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; water; dihydrogen peroxide; quinuclidine hydrochloride; potassium carbonate; periodic acid; potassium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; formic acid; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja408034x

Reference yield:

: 1383117-23-4
C₂₃H₃₀N₂O₁₀

: 1383254-81-6
C₃₅H₃₈N₂O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrazine hydrate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

1.2: 0.75 h / 0 °C / Inert atmosphere

2.1: trifluoroacetic acid / 2,2,2-trifluoroethanol / 1.5 h / 20 °C

2.2: 0.83 h / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / 1,4-dioxane / 1.5 h / 100 °C

4.1: hydrogenchloride / ethyl acetate / 0.5 h / 20 °C

4.2: 1 h / 0 °C

5.1: L-Selectride / tetrahydrofuran / 1 h / -42 °C

5.2: 5 h / Reflux

6.1: potassium hydroxide / 1,4-dioxane; water / 1 h / 20 °C

6.2: 0.17 h / 0 °C

7.1: tert.-butylnitrite; boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / -15 - 0 °C / Inert atmosphere

7.2: 1 h / 0 - 20 °C

8.1: quinuclidine hydrochloride; methanesulfonamide; potassium hexacyanoferrate(III); osmium(VIII) oxide / water; tert-butyl alcohol / 39 h / 20 °C

9.1: periodic acid / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; potassium phosphate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tert.-butylnitrite; methanesulfonamide; boron trifluoride diethyl etherate; quinuclidine hydrochloride; L-Selectride; hydrazine hydrate; periodic acid; trifluoroacetic acid; potassium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; 1,4-dioxane; 2,2,2-trifluoroethanol; water; ethyl acetate; tert-butyl alcohol; 3.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ja408034x