2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide

Base Information

Chemical Name:2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide
CAS No.:1309191-68-1
Molecular Formula:C₂₄H₂₅N₃O₂S
Molecular Weight:419.547
Hs Code.:

Synonyms:2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide

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Chemical Property of 2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide

Chemical Property:

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Technology Process of 2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide

There total 4 articles about 2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19835-38-2
1-adamantylacetyl chloride

: 1309195-34-3
5-amino-7-phenylthieno[2,3-d]pyridazin-4(5H)-one

: 1309191-68-1
2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide

Guidance literature:: With pyridine; In dichloromethane; for 2h;

Reference yield:

: 88-13-1
3-Thiophene carboxylic acid

: 1309191-68-1
2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.08 h / 0 °C

1.3: 7 h / 80 °C

2.1: potassium tert-butylate / tetrahydrofuran / 1 h

2.2: 1 h

3.1: pyridine / dichloromethane / 2 h

With pyridine; n-butyllithium; potassium tert-butylate; diisopropylamine; In tetrahydrofuran; hexanes; dichloromethane;

Reference yield:

: 93-97-0
benzoic acid anhydride

: 1309191-68-1
2-(1-adamantyl)-N-(4-oxo-7-phenylthieno[2,3-d]pyridazin-5(4H)-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.08 h / 0 °C

1.3: 7 h / 80 °C

2.1: potassium tert-butylate / tetrahydrofuran / 1 h

2.2: 1 h

3.1: pyridine / dichloromethane / 2 h

With pyridine; n-butyllithium; potassium tert-butylate; diisopropylamine; In tetrahydrofuran; hexanes; dichloromethane;