C₃₀H₃₆N₂O

Base Information

• Chemical Name: C₃₀H₃₆N₂O
• CAS No.: 210552-30-0
• Molecular Formula: C₃₀H₃₆N₂O
• Molecular Weight: 440.629

Synonyms:C₃₀H₃₆N₂O

Chemical Property of C₃₀H₃₆N₂O

Chemical Property:

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Technology Process of C₃₀H₃₆N₂O

There total 6 articles about C₃₀H₃₆N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-4-heptene (143064-98-6) + (6S,10S,8E)-12-Benzyl-5-methyl-6,7,10,11-tetrahydro-6,10-epimino-5H-cyclooctindole-9-carbaldehyde (143120-74-5) → (-)-(6S,10S)-5-methyl-9-(2'-ethyl-1'-hydroxy-3'-hexenyl)-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooct[b]indole (143064-99-7) + C30H36N2O (210552-30-0)

Guidance literature:

With magnesium; In tetrahydrofuran; at 0 ℃; Yield given. Yields of byproduct given;

DOI:10.1021/jo980476p

Reference yield:

(6S,10S)-(-)-5-methyl-9-oxo-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctaindole (123806-87-1) → C30H36N2O (210552-30-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) LDA, KOH, 2.) LiClO₄ / 2.) dioxane, reflux

2: Mg / tetrahydrofuran / 0 °C

With potassium hydroxide; lithium perchlorate; magnesium; lithium diisopropyl amide; In tetrahydrofuran;

DOI:10.1021/jo980476p

Reference yield:

benzaldehyde (100-52-7) → C30H36N2O (210552-30-0)

Guidance literature:

Multi-step reaction with 5 steps

1: methanol / 2 h / Ambient temperature

2: 1.) NaBH₄, 2.) TFA / 1.) -30 - -10 deg C, 3 h, 2.) CHCl₃, reflux, 12 h

3: 1.) NaH, 2.) HCl / 1.) CH₃OH, PhCH₃, reflux, 4 h, 2.) HOAc, reflux, 12 h

4: 1.) LDA, KOH, 2.) LiClO₄ / 2.) dioxane, reflux

5: Mg / tetrahydrofuran / 0 °C

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; lithium perchlorate; sodium hydride; magnesium; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; methanol;

DOI:10.1021/jo980476p

upstream raw materials:

3-bromo-4-heptene

(6S,10S,8E)-12-Benzyl-5-methyl-6,7,10,11-tetrahydro-6,10-epimino-5H-cyclooctindole-9-carbaldehyde

(6S,10S)-(-)-5-methyl-9-oxo-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctaindole

benzaldehyde

Downstream raw materials:

C₃₂H₄₀N₂O₂

(-)-(6S,8S,9S,10S,1'R)-5-methyl-8-(1'-ethyl-2'-oxoethyl)-9-(1',3'-dioxolan-2'-yl)-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooct[b]indole

(6S,8S,9S,10S,1'S)-5-methyl-8-(1'-ethyl-oxomethyl)-9-(1',3'-dioxolan-2'-yl)-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooct[b]-indole

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