PROPANEDIOIC ACID (2-THIENYL METHYLENE)DIMETHYL ESTER

Base Information

Chemical Name:PROPANEDIOIC ACID (2-THIENYL METHYLENE)DIMETHYL ESTER
CAS No.:72796-68-0
Molecular Formula:C10H10 O4 S
Molecular Weight:226.253
Hs Code.:
Mol file:72796-68-0.mol

Synonyms:Propanedioicacid, (2-thienylmethylene)-, dimethyl ester (9CI)

Suppliers and Price of PROPANEDIOIC ACID (2-THIENYL METHYLENE)DIMETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of PROPANEDIOIC ACID (2-THIENYL METHYLENE)DIMETHYL ESTER

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of PROPANEDIOIC ACID (2-THIENYL METHYLENE)DIMETHYL ESTER

There total 1 articles about PROPANEDIOIC ACID (2-THIENYL METHYLENE)DIMETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 98-03-3
thiophene-2-carbaldehyde

: 6773-29-1
dimethyl diazomalonate

: 72796-68-0
dimethyl 2‐(thiophen‐2‐ylmethylene)malonate

Guidance literature:: With tributylstibine; copper(l) iodide; In benzene; at 70 ℃; for 4h;
DOI:10.1016/S0040-4039(00)97988-7

Reference yield: 95.0%

: 106595-91-9
4-benzyl-3,4-dihydroquinoxalin-2(1H)-one

: 72796-68-0
dimethyl 2‐(thiophen‐2‐ylmethylene)malonate

: dimethyl 2‐((1‐benzyl‐3‐oxo‐1,2,3,4‐tetrahydroquinoxalin‐2‐yl)(thiophen‐2‐yl)methyl)malonate

Guidance literature:: With diphenyl hydrogen phosphate; tris(bipyridine)ruthenium(II) dichloride hexahydrate; In acetonitrile; at 20 ℃; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.0c02953

Reference yield: 81.0%

: 66073-33-4
4-(2-nitrophenyl)-3-oxobutyric acid ethyl ester

: 72796-68-0
dimethyl 2‐(thiophen‐2‐ylmethylene)malonate

: C₂₂H₂₃NO₉S

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 60 ℃; for 22h; diastereoselective reaction;
DOI:10.1039/c5ra01430a