cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

Base Information

Chemical Name:cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane
CAS No.:471930-32-2
Molecular Formula:C₁₄H₁₈Si
Molecular Weight:214.382
Hs Code.:

Synonyms:cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

Suppliers and Price of cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

There total 1 articles about cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1165952-92-0
cyclohexa-1,4-diene

: 768-33-2
phenyldimethylsilyl chloride

: 471930-32-2
cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

Guidance literature:: cyclohexa-1,4-diene; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -45 ℃; for 2.5h;

phenyldimethylsilyl chloride; In tetrahydrofuran; cyclohexane; at -45 ℃; for 0.5h; Further stages.;
DOI:10.1021/ja012152f

Reference yield: 94.0%

: 530-48-3
1,1-Diphenylethylene

: 471930-32-2
cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

: (2,2-diphenylethyl)dimethyl(phenyl)silane

Guidance literature:: With tris(pentafluorophenyl)borate; In dichloromethane; at 20 ℃; for 24h; Glovebox; Inert atmosphere;
DOI:10.1002/anie.201305584

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 471930-32-2
cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane

: (1S,4R,5R)-4-(Dimethyl-phenyl-silanyl)-6-aza-bicyclo[3.2.1]oct-2-en-7-one

: rac-(1R,5R,8R)-8-dimethylphenylsilyl-6-azabicyclo[3.2.1]oct-3-en-7-one

Guidance literature:: isocyanate de chlorosulfonyle; cyclohexa-2,5-dien-1-yldimethyl(phenyl)silane; In dichloromethane; at -45 ℃; for 13h;

With 25percent aq. Na₂SO₃; In dichloromethane; at 23 ℃; for 22h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ja012152f