1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde

Base Information

Chemical Name:1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde
CAS No.:77664-95-0
Molecular Formula:C12H11 Cl O2
Molecular Weight:222.671
Hs Code.:2913000090
DSSTox Substance ID:DTXSID70445747
Wikidata:Q82264273
Mol file:77664-95-0.mol

Synonyms:77664-95-0;1-chloro-7-methoxy-3,4-dihydronaphthalene-2-carbaldehyde;1-CHLORO-7-METHOXY-3,4-DIHYDRO-NAPHTHALENE-2-CARBALDEHYDE;SCHEMBL6832547;DTXSID70445747;CDA66495;AC8626;MFCD07371509;AKOS017560361;SB38726;SY264264;FT-0714475

Suppliers and Price of 1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde 97%
5g
$ 3998.00

J&W Pharmlab
1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde 97%
1g
$ 998.00

J&W Pharmlab
1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde 97%
500mg
$ 549.00

Crysdot
1-Chloro-7-methoxy-3,4-dihydronaphthalene-2-carbaldehyde 95+%
1g
$ 445.00

Chemenu
1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde 95%
1g
$ 420.00

American Custom Chemicals Corporation
1-CHLORO-7-METHOXY-3,4-DIHYDRO-NAPHTHALENE-2-CARBALDEHYDE 95.00%
5MG
$ 503.86

Alichem
1-Chloro-7-methoxy-3,4-dihydronaphthalene-2-carbaldehyde
1g
$ 388.41

AK Scientific
1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde
1g
$ 694.00

Total 10 raw suppliers

Chemical Property of 1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde

Chemical Property:

PSA：26.30000
LogP:2.79020
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:222.0447573
Heavy Atom Count:15
Complexity:285

Purity/Quality:

97% ^*data from raw suppliers

1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=C(CCC(=C2Cl)C=O)C=C1

Technology Process of 1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde

There total 2 articles about 1-Chloro-7-methoxy-3,4-dihydro-naphthalene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.1%

: 6836-19-7
7-Methoxy-1-tetralone

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 77664-95-0
1-chloro-7-methoxy-3,4-dihydronaphthalene-2-carboxaldehyde

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; for 0.5h; Cooling with ice;

7-Methoxy-1-tetralone; at 20 - 70 ℃; for 2h;

Reference yield:

: 77664-95-0
1-chloro-7-methoxy-3,4-dihydronaphthalene-2-carboxaldehyde

Guidance literature:

Reference yield: 93.0%

: 77664-95-0
1-chloro-7-methoxy-3,4-dihydronaphthalene-2-carboxaldehyde

: 98-80-6
phenylboronic acid

: 7-methoxy-1-phenyl-3,4-dihydronaphthalene-2-carbaldehyde

Guidance literature:: With tetrabutylammomium bromide; palladium diacetate; potassium carbonate; In 1,4-dioxane; water; at 45 ℃; for 1h;
DOI:10.1021/jacs.6b07424