(6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone

Base Information

Chemical Name:(6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone
CAS No.:229009-99-8
Molecular Formula:C₃₂H₂₉N₃O₉
Molecular Weight:599.597
Hs Code.:

Synonyms:(6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone

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Chemical Property of (6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone

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Technology Process of (6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone

There total 2 articles about (6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 563-41-7
semicarbazide hydrochloride

: 229009-97-6
(6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one

: 229009-99-8
(6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone

Guidance literature:: In 1,4-dioxane; at 20 ℃; for 1.5h;
DOI:10.1016/S0008-6215(98)00307-3

Reference yield:

: 121701-32-4
6-hydroxy-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3<2H,6H>-one

: 229009-99-8
(6S)-6-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyran-3(2H,6H)-one semicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / Et₃SiH; BF₃*Et₂O / acetonitrile / 0.01 h / 0 °C

2: 80 percent / dioxane / 1.5 h / 20 °C

With triethylsilane; boron trifluoride diethyl etherate; In 1,4-dioxane; acetonitrile; 1: Reduction / 2: Condensation;
DOI:10.1016/S0008-6215(98)00307-3