1,1a(2)-(3-Bromo-1-propen-1-ylidene)bis[4-iodobenzene]

Base Information

Chemical Name:1,1a(2)-(3-Bromo-1-propen-1-ylidene)bis[4-iodobenzene]
CAS No.:869015-09-8
Molecular Formula:C₁₅H₁₁BrI₂
Molecular Weight:524.965
Hs Code.:
DSSTox Substance ID:DTXSID701225939

Synonyms:SCHEMBL1245252;DTXSID701225939;AKOS005216765;869015-09-8;1,1a(2)-(3-Bromo-1-propen-1-ylidene)bis[4-iodobenzene]

Suppliers and Price of 1,1a(2)-(3-Bromo-1-propen-1-ylidene)bis[4-iodobenzene]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,1a(2)-(3-Bromo-1-propen-1-ylidene)bis[4-iodobenzene]

Chemical Property:

XLogP3:6.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:523.81336
Heavy Atom Count:18
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=CCBr)C2=CC=C(C=C2)I)I

Technology Process of 1,1a(2)-(3-Bromo-1-propen-1-ylidene)bis[4-iodobenzene]

There total 2 articles about 1,1a(2)-(3-Bromo-1-propen-1-ylidene)bis[4-iodobenzene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5630-56-8
4,4'-diiodobenzophenone

: 869015-09-8
3,3-bis(4-iodophenyl)allyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; ethylene dibromide / tetrahydrofuran / 0.5 h

1.2: 0.5 h / Reflux

1.3: 0.5 h

2.1: trimethylsilyl bromide / dichloromethane / 0 °C

With trimethylsilyl bromide; magnesium; ethylene dibromide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 673479-16-8
ethyl 3,3-bis-(4-iodophenyl)-acrylate

: 869015-09-8
3,3-bis(4-iodophenyl)allyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 48 h / -10 - 20 °C / Inert atmosphere

2: trimethylsilyl bromide / dichloromethane / 0 °C

With trimethylsilyl bromide; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane;