C₄₅H₃₉N₃O₅

Base Information

• Chemical Name: C₄₅H₃₉N₃O₅
• CAS No.: 1417604-13-7
• Molecular Formula: C₄₅H₃₉N₃O₅
• Molecular Weight: 701.822
• Mol file: 1417604-13-7.mol

Synonyms:C₄₅H₃₉N₃O₅

Chemical Property of C₄₅H₃₉N₃O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₃₉N₃O₅

There total 3 articles about C₄₅H₃₉N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C38H30N2O5 + benzylamine (100-46-9) → C45H39N3O5 (1417604-13-7) + C45H39N3O5 (1417604-14-8)

Guidance literature:

With lithium perchlorate; In acetonitrile; at 20 ℃; for 1h;

DOI:10.1016/j.bmcl.2012.11.011

Reference yield:

C36H27BrN2O4 (1417604-08-0) → C45H39N3O5 (1417604-13-7)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / Reflux

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C

3: lithium perchlorate / acetonitrile / 1 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium perchlorate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene; acetonitrile;

DOI:10.1016/j.bmcl.2012.11.011

Reference yield:

N-Fmoc-D-phenylglycine (111524-95-9,163883-97-4) → C45H39N3O5 (1417604-13-7)

Guidance literature:

Multi-step reaction with 4 steps

1: triphenylphosphine; 1,1,1,3,3,3-hexachloro-propan-2-one / dichloromethane / 0.58 h / -10 - 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / Reflux

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C

4: lithium perchlorate / acetonitrile / 1 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,1,1,3,3,3-hexachloro-propan-2-one; lithium perchlorate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In dichloromethane; toluene; acetonitrile;

DOI:10.1016/j.bmcl.2012.11.011

upstream raw materials:

benzylamine

N-Fmoc-D-phenylglycine

C₃₆H₂₇BrN₂O₄

Downstream raw materials:

C₃₀H₂₉N₃O₃

C₃₀H₂₇N₃O₂

Refernces