3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin

Base Information

Chemical Name:3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin
CAS No.:66065-91-6
Molecular Formula:C₂₅H₄₀N₄O₁₁
Molecular Weight:572.613
Hs Code.:

Synonyms:3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin

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Technology Process of 3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin

There total 1 articles about 3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 66065-86-9
3,2',6'-tri-N-acetylsisomicin

: 66065-91-6
3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin

Guidance literature:: With sulfuric acid; 3,5-di-tert-butyl-o-benzoquinone; In methanol; at 25 ℃; for 40h; pH = 3;
DOI:10.1039/P19810002168

Reference yield:

: 66065-91-6
3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin

: 56391-56-1
netilmicin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen chloride, sodium cyanoborohydride / methanol / 1.) pH = 5.5, 25 deg C, 7 h, 2.) 25 deg C, 18 h

2: 10 percent / 5percent aq. sodium hydroxide / 50 h / Heating

With hydrogenchloride; sodium hydroxide; sodium cyanoborohydride; In methanol;
DOI:10.1039/P19810002168

Reference yield:

: 66065-91-6
3,2',6'-tri-N-acetyl-1-deamino-1-oxosisomicin

: 32385-11-8
sisomicin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen chloride, sodium cyanoborohydride / methanol / 1.) pH = 5.5, 25 deg C, 7 h, 2.) 25 deg C, 18 h

2: 4 percent / 5percent aq. sodium hydroxide / 50 h / Heating

With hydrogenchloride; sodium hydroxide; sodium cyanoborohydride; In methanol;
DOI:10.1039/P19810002168