Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2CF₃SO₃

Base Information

• Chemical Name: Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2CF₃SO₃
• CAS No.: 470663-75-3
• Molecular Formula: CF₃O₃S*C₄₂H₃₆IrO₂P₂
• Molecular Weight: 975.985

Synonyms:Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2CF₃SO₃

Chemical Property of Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2CF₃SO₃

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Technology Process of Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2CF₃SO₃

There total 1 articles about Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2CF₃SO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Ir(CHCH2)2(CH3CN)2(P(C6H5)3)2(1+)*CF3SO3(1-)=Ir(CHCH2)2(CH3CN)2(P(C6H5)3)2CF3SO3 (470663-73-1) + carbon monoxide (201230-82-2) → Ir(CHCH2)2(CO)2(P(C6H5)3)2(1+)*CF3SO3(1-)=Ir(CHCH2)2(CO)2(P(C6H5)3)2CF3SO3 (470663-75-3)

Guidance literature:

In dichloromethane; byproducts: CH3CN; Ir-complex in CH2Cl2 was stirred under CO (1 atm) at 25°C for 3 h, n-pentane was added; filtered, washed with n-pentane, dried under vac.; elem. anal.;

DOI:10.1021/om020410r

Reference yield: 82.0%

Ir(CHCH2)2(CO)2(P(C6H5)3)2(1+)*CF3SO3(1-)=Ir(CHCH2)2(CO)2(P(C6H5)3)2CF3SO3 (470663-75-3) + phenylacetylene (536-74-3) → Ir(CCC6H5)(CHCH2)2(CO)(P(C6H5)3)2 (470663-84-4)

Guidance literature:

With Me₃NO; In chloroform; byproducts: CO2, NHMe3OTf; Me3NO was added to soln. of Ir-complex and ligand in CHCl3, stirred at 25°C for 30 min under N2; extd. with H2O, n-pentane was added, filtered, washed with n-pentane, dried under vac.; elem. anal.;

DOI:10.1021/om020410r

Reference yield: 74.0%

Ir(CHCH2)2(CO)2(P(C6H5)3)2(1+)*CF3SO3(1-)=Ir(CHCH2)2(CO)2(P(C6H5)3)2CF3SO3 (470663-75-3) + 1,4-diethynylbenzene (935-14-8) → C6H4(IrC2(CHCH2)2(CO)(P(C6H5)3)2)2

Guidance literature:

With Me₃NO; In chloroform; byproducts: CO2, NHMe3OTf; Me3NO was added to soln. of Ir-complex and ligand in CHCl3, kept at 25°C for 2 h under N2; extd. with water, n-pentane was added, filtered, washed with MeOH, driedunder vac.; elme. anal.;

DOI:10.1021/om020410r

upstream raw materials:

Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2CF₃SO₃

carbon monoxide

Downstream raw materials:

Ir(CCC₆H₉)(CHCH₂)2(CO)(P(C₆H₅)3)2

Ir(CCC₆H₅)(CHCH₂)2(CO)(P(C₆H₅)3)2

Ir(CCC₆H₄CH₃)(CHCH₂)2(CO)(P(C₆H₅)3)2

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