Technology Process of C19H21(18)FN4O3S
There total 7 articles about C19H21(18)FN4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate; [2.2.2]cryptande;
In
dimethyl sulfoxide; acetonitrile;
at 100 ℃;
for 0.25h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dimethyl sulfoxide / 16 h / 20 °C
2: methanesulfonic acid; L-methionine / 72 h
3: caesium carbonate / N,N-dimethyl-formamide / 15 h
4: [2.2.2]cryptande; potassium carbonate / dimethyl sulfoxide; acetonitrile / 0.25 h / 100 °C / Inert atmosphere
With
methanesulfonic acid; L-methionine; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; N-ethyl-N,N-diisopropylamine; [2.2.2]cryptande;
In
dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: caesium carbonate / N,N-dimethyl-formamide / 15 h
2: [2.2.2]cryptande; potassium carbonate / dimethyl sulfoxide; acetonitrile / 0.25 h / 100 °C / Inert atmosphere
With
potassium carbonate; caesium carbonate; [2.2.2]cryptande;
In
dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;