C₁₆H₁₈O

Base Information

Chemical Name:C₁₆H₁₈O
CAS No.:1334512-22-9
Molecular Formula:C₁₆H₁₈O
Molecular Weight:226.318
Hs Code.:

Synonyms:C₁₆H₁₈O

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Chemical Property of C₁₆H₁₈O

Chemical Property:

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Technology Process of C₁₆H₁₈O

There total 4 articles about C₁₆H₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1334667-17-2
C₁₆H₁₆

: 1334512-22-9
C₁₆H₁₈O

Guidance literature:: C₁₆H₁₆; With borane-dimethyl sulfide complex; In tetrahydrofuran; at 0 - 20 ℃; for 1.16667h;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 1h;
DOI:10.1002/anie.201103581

Reference yield:

: 501922-06-1
(E)-3-(2-methylphenyl)-2-propenol

: 1334512-22-9
C₁₆H₁₈O

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; triethylamine / dichloromethane / 9 h / 0 - 20 °C

2.1: C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; copper(l) chloride / tetrahydrofuran / 16 h / 30 °C

3.1: borane-dimethyl sulfide complex / tetrahydrofuran / 1.17 h / 0 - 20 °C

3.2: 1 h / 0 - 20 °C

With dmap; borane-dimethyl sulfide complex; C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; triethylamine; copper(l) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201103581

Reference yield:

: 768392-27-4
diethyl (E)-3-(2-methylphenyl)prop-2-enyl phosphate

: 1334512-22-9
C₁₆H₁₈O

Guidance literature:: Multi-step reaction with 2 steps

1.1: C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; copper(l) chloride / tetrahydrofuran / 16 h / 30 °C

2.1: borane-dimethyl sulfide complex / tetrahydrofuran / 1.17 h / 0 - 20 °C

2.2: 1 h / 0 - 20 °C

With borane-dimethyl sulfide complex; C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; copper(l) chloride; In tetrahydrofuran;
DOI:10.1002/anie.201103581