4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one

Base Information

• Chemical Name: 4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one
• CAS No.: 80413-03-2
• Molecular Formula: C₃₀H₂₀N₂O₄
• Molecular Weight: 472.5

Synonyms:4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one

Chemical Property of 4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one

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Technology Process of 4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one

There total 3 articles about 4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-<(2',3'-diphenyl-6'-methoxy-5'-benzofuranyl)methylene>-2-phenyloxazolin-5-one (80412-97-1) → 4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one (80413-03-2)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 5h; Heating;

DOI:10.1002/jhet.5570180628

Reference yield:

Hippuric Acid (495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2) → 4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one (80413-03-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / anhydrous sodium acetate / acetic anhydride / 2 h / 100 °C

2: 65 percent / hydroxylamine hydrochloride / ethanol / 5 h / Heating

With hydroxylamine hydrochloride; sodium acetate; In ethanol; acetic anhydride;

DOI:10.1002/jhet.5570180628

Reference yield:

2,3-diphenyl-5-formyl-6-methoxybenzofuran (54525-60-9) → 4-<(2',3'-diphenyl-6'-methoxy-5'benzofuranyl)methylene>-1-hydroxy-2-phenyl-5H-imidazolin-5-one (80413-03-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / anhydrous sodium acetate / acetic anhydride / 2 h / 100 °C

2: 65 percent / hydroxylamine hydrochloride / ethanol / 5 h / Heating

With hydroxylamine hydrochloride; sodium acetate; In ethanol; acetic anhydride;

DOI:10.1002/jhet.5570180628

upstream raw materials:

4-<(2',3'-diphenyl-6'-methoxy-5'-benzofuranyl)methylene>-2-phenyloxazolin-5-one

Hippuric Acid

2,3-diphenyl-5-formyl-6-methoxybenzofuran

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