((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester

Base Information

Chemical Name:((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester
CAS No.:141521-16-6
Molecular Formula:C₁₂H₁₉NO₂
Molecular Weight:209.288
Hs Code.:

Synonyms:((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester

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Chemical Property of ((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester

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Technology Process of ((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester

There total 4 articles about ((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 598-55-0
methyl carbamate

: 350049-01-3
trans-1-(phenylseleno)-5-isopropenyl-2-methylcyclohex-2-ene

: 141521-16-6
((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester

Guidance literature:: With N-chloro-succinimide; N-ethyl-N,N-diisopropylamine; In methanol; at 20 ℃; for 24h;

Reference yield:

: 7632-16-8,22567-18-6,20307-86-2
(2S,4S)-carveol

: 141521-16-6
((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / diisopropyl azodicarboxylate, PH₃P / tetrahydrofuran / 0 °C

2: hydrazine hydrate / ethanol / Heating

3: Et₃N / CH₂Cl₂ / Ambient temperature

With di-isopropyl azodicarboxylate; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1246/cl.1992.443

Reference yield:

: 141521-15-5
2-((1S,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-isoindole-1,3-dione

: 141521-16-6
((1R,5S)-5-Isopropenyl-2-methyl-cyclohex-2-enyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / Heating

2: Et₃N / CH₂Cl₂ / Ambient temperature

With hydrazine hydrate; triethylamine; In ethanol; dichloromethane;
DOI:10.1246/cl.1992.443