oxo(tetra-p-tolylporphinato)chromium(IV)

Base Information

Chemical Name:oxo(tetra-p-tolylporphinato)chromium(IV)
CAS No.:78833-34-8
Molecular Formula:C₅₀H₄₄CrN₄O
Molecular Weight:768.922
Hs Code.:

Synonyms:oxo(tetra-p-tolylporphinato)chromium(IV)

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Chemical Property of oxo(tetra-p-tolylporphinato)chromium(IV)

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Technology Process of oxo(tetra-p-tolylporphinato)chromium(IV)

There total 32 articles about oxo(tetra-p-tolylporphinato)chromium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 28110-70-5
chloro(5,10,15,20-tetraphenylporphyrinato)chromium(III)

: 78833-34-8
(5,10,15,20-tetraphenylporphyrinato)oxochromium(IV)

: 72260-61-8
{OCr(C₄₄H₂₈N₄)Cl}

Guidance literature:: With 4-cyano-N,N-dimethylaniline-N-oxide; In dichloromethane; Irradiation (UV/VIS); irrdn. of CH2Cl2 soln. contg. (TPP)CrCl (1E-4 M) and N-oxide (1.2E-3 M) by diffuse room fluorescent light for 2 min; not isolated; detected by UV;
DOI:10.1021/ja00312a083

Reference yield: 80.0%

: 28110-70-5
chloro(5,10,15,20-tetraphenylporphyrinato)chromium(III)

: 78833-34-8
(5,10,15,20-tetraphenylporphyrinato)oxochromium(IV)

Guidance literature:: With oxygen; In tetrahydrofuran; evapd. in vac., extrd. with hot deoxygenated toluene, filtered, exposedto air;
DOI:10.1039/c39810000370

Reference yield: 68.0%

: 33519-59-4
CrOH(C₂₂H₁₂N₄)(C₆H₅CH₃)4*2H₂O

: 78833-34-8
oxo(tetra-p-tolylporphinato)chromium(IV)

Guidance literature:: With sodium hydroxide; sodium hypochlorite; In ethanol; dichloromethane; reaction mixt. was stirred until the color changed to red; washing with 2 M NaOH, then dried in vac., the residue was chromd. at basic alumina with CH2Cl2. The first red fraction was evapd., then recrystd. from benzene, washed with acetone; elem. anal.;
DOI:10.1021/ic00132a078