8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one

Base Information

Chemical Name:8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one
CAS No.:138452-36-5
Molecular Formula:C₃₅H₂₆ClNO₂
Molecular Weight:528.05
Hs Code.:

Synonyms:8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one

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Chemical Property of 8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one

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Technology Process of 8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one

There total 4 articles about 8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 117-11-3
1-amino-5-chloroanthracene-9,10-dione

: 100-44-7
benzyl chloride

: 138452-36-5
8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 30 ℃; for 1h;
DOI:10.1246/bcsj.64.3417

Reference yield:

: 82-50-8
5-nitroanthraquinone-1-sulfonic acid

: 138452-36-5
8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: HCl, NaClO₄

2: Na₂S, aq. NaOH / 10 h / 80 °C

3: 53 percent / KOH / dimethylsulfoxide / 1 h / 30 °C

With hydrogenchloride; sodium sulfide; potassium hydroxide; sodium hydroxide; sodium perchlorate; In dimethyl sulfoxide;
DOI:10.1246/bcsj.64.3417

Reference yield:

: 129-40-8
5-chloro-1-nitroanthraquinone

: 138452-36-5
8-Chloro-3,11b-dibenzyl-2-phenyl-3,11b-dihydroanthra<1,9-de>-1,3-oxazin-7(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂S, aq. NaOH / 10 h / 80 °C

2: 53 percent / KOH / dimethylsulfoxide / 1 h / 30 °C

With sodium sulfide; potassium hydroxide; sodium hydroxide; In dimethyl sulfoxide;
DOI:10.1246/bcsj.64.3417