1-chloro-2,3,4,5-tetraethyl-1-stibole

Base Information

• Chemical Name: 1-chloro-2,3,4,5-tetraethyl-1-stibole
• CAS No.: 278169-24-7
• Molecular Formula: C₁₂H₂₀ClSb
• Molecular Weight: 321.494

Synonyms:1-chloro-2,3,4,5-tetraethyl-1-stibole

Chemical Property of 1-chloro-2,3,4,5-tetraethyl-1-stibole

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Technology Process of 1-chloro-2,3,4,5-tetraethyl-1-stibole

There total 1 articles about 1-chloro-2,3,4,5-tetraethyl-1-stibole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,1-bis(cyclopentadienyl)-2,3,4,5-tetraethyl-1-zircona-cyclopenta-2,4-diene + antimony(III) chloride (10025-91-9) → zirconocene dichloride (1291-32-3) + 1-chloro-2,3,4,5-tetraethyl-1-stibole (278169-24-7)

Guidance literature:

In tetrahydrofuran; under Ar atm. SbCl3 was added to soln. 1,1-bis(cyclopentadienyl)-2,3,4,5-tetraethyl-1-zirconacyclopenta-2,4-diene in THF and stirred for 24 h at room temp.; volatile materials were removed under vac., residue was extd. with pentane, solvent was removed; elem. anal.;

DOI:10.1021/om000161b

upstream raw materials:

antimony(III) chloride

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