4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol

Base Information

• Chemical Name: 4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol
• CAS No.: 1260153-11-4
• Molecular Formula: C₁₈H₂₄O₃
• Molecular Weight: 288.387

Synonyms:4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol

Chemical Property of 4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol

Chemical Property:

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Technology Process of 4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol

There total 3 articles about 4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

(+)-Δ3-carene (498-15-7,19079-29-9) + vanillin (121-33-5,8014-42-4) → 4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol (1260153-11-4) + 4-[(1R,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol (1260153-18-1) + 2-methoxy-4-(4,4,8-trimethyl-3-oxabicyclo[3.3.1]non-7-en-2-yl)phenol

Guidance literature:

With montmorillonite K₁₀ clay; In dichloromethane; at 20 ℃; for 96h; optical yield given as %ee;

DOI:10.1002/hlca.201000145

Reference yield: 4.0%

2-carene (4497-92-1) + vanillin (121-33-5,8014-42-4) → 4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol (1260153-11-4) + 4-[(1R,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol (1260153-18-1) + 2-methoxy-4-(4,4,8-trimethyl-3-oxabicyclo[3.3.1]non-7-en-2-yl)phenol

Guidance literature:

With montmorillonite K₁₀ clay; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1002/hlca.201000145

Reference yield:

2-carene (554-61-0) + vanillin (121-33-5,8014-42-4) → 4-[(1S,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol (1260153-11-4) + 4-[(1R,3aR,7aS)-1,3,3a,4,5,7a-hexahydro-3,3,6-trimethylisobenzofuran-1-yl]-2-methoxyphenol (1260153-18-1) + C18H24O3

Guidance literature:

With montmorillonite clay K₁₀; In neat (no solvent); at 20 ℃; for 20h;

DOI:10.3390/molecules25153496

upstream raw materials:

(+)-Δ³-carene

vanillin

2-carene

2-carene

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