trans-N,N-diethyl-o-aminocinnamamide

Base Information

Chemical Name:trans-N,N-diethyl-o-aminocinnamamide
CAS No.:440640-39-1
Molecular Formula:C₁₃H₁₈N₂O
Molecular Weight:218.299
Hs Code.:

Synonyms:trans-N,N-diethyl-o-aminocinnamamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-N,N-diethyl-o-aminocinnamamide

Chemical Property:

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Technology Process of trans-N,N-diethyl-o-aminocinnamamide

There total 1 articles about trans-N,N-diethyl-o-aminocinnamamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 440640-37-9
(E)-N,N-diethyl-3-(2-nitrophenyl)acrylamide

: 440640-39-1
trans-N,N-diethyl-o-aminocinnamamide

Guidance literature:: With hydrazine hydrate; palladium on activated charcoal; In ethanol; for 1h; Heating;
DOI:10.1002/jhet.5570390108

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 440640-39-1
trans-N,N-diethyl-o-aminocinnamamide

: C₂₂H₂₄N₂O

Guidance literature:: With magnesium sulfate; sodium sulfate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.joc.6b01621

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 440640-39-1
trans-N,N-diethyl-o-aminocinnamamide

: (E)-N,N-diethyl-2-(2-styryl-1H-indol-3-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate; magnesium sulfate / tetrahydrofuran / 20 °C / Inert atmosphere

2: sodium cyanide / N,N-dimethyl-formamide / 60 °C / Inert atmosphere; Molecular sieve

With sodium cyanide; magnesium sulfate; sodium sulfate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/acs.joc.6b01621