methyl imidazo[1,2-a]pyridine-2-carboxylate

Base Information

• Chemical Name: methyl imidazo[1,2-a]pyridine-2-carboxylate
• CAS No.: 1220397-13-6
• Molecular Formula: C₉H₈N₂O₂
• Molecular Weight: 176.175
• Hs Code.: 2933998090

Synonyms:methyl imidazo[1,2-a]pyridine-2-carboxylate

Chemical Property of methyl imidazo[1,2-a]pyridine-2-carboxylate

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

MethylImidazo[1,2-a]pyridine-2-carboxylate ^*data from reagent suppliers

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Technology Process of methyl imidazo[1,2-a]pyridine-2-carboxylate

There total 1 articles about methyl imidazo[1,2-a]pyridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

pyridine (110-86-1) + C6H9NO4 (1492880-24-6) → methyl imidazo[1,2-a]pyridine-2-carboxylate (1220397-13-6)

Guidance literature:

With copper(l) iodide; lithium carbonate; In N,N-dimethyl-formamide; at 95 ℃; for 2h;

DOI:10.1021/ol403105p

Reference yield: 86.0%

2-bromo-p-toluidine (583-68-6) + methyl imidazo[1,2-a]pyridine-2-carboxylate (1220397-13-6) → N-(2-bromo-4-methylphenyl)-imidazo[1,2-a]pyridine-2-carboxamide (924206-88-2)

Guidance literature:

2-bromo-p-toluidine; With trimethylaluminum; In dichloromethane; toluene; at -5 - 0 ℃; Inert atmosphere;

methyl imidazo[1,2-a]pyridine-2-carboxylate; In dichloromethane; toluene; at 0 ℃; Reflux; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; toluene; at 0 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.12.049

upstream raw materials:

pyridine

C₆H₉NO₄

Downstream raw materials:

N-(2-bromo-4-methylphenyl)-imidazo[1,2-a]pyridine-2-carboxamide

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