3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester

Base Information

Chemical Name:3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester
CAS No.:627537-06-8
Molecular Formula:C₁₉H₂₈O₃S
Molecular Weight:336.496
Hs Code.:

Synonyms:3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester

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Chemical Property of 3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester

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Technology Process of 3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester

There total 1 articles about 3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57768-35-1
1-(phenylthio)-1-cyclohexanecarboxaldehyde

: 97-62-1
Ethyl isobutyrate

: 627537-06-8
3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester

Guidance literature:: Ethyl isobutyrate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

1-(phenylthio)-1-cyclohexanecarboxaldehyde; In tetrahydrofuran; Further stages.;
DOI:10.1039/b303790h

Reference yield: 93.0%

: 627537-06-8
3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester

: 627537-07-9
2,2-dimethyl-1-(1-phenylsulfanyl-cyclohexyl)-propane-1,3-diol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1039/b303790h

Reference yield:

: 627537-06-8
3-hydroxy-2,2-dimethyl-3-(1-phenylsulfanyl-cyclohexyl)-propionic acid ethyl ester

: 3,3-dimethyl-4-phenylsulfanyl-1-oxa-spiro[4.5]decane

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / LiAlH₄ / diethyl ether

2: acetonitrile

3: SiO₂ / 20 °C

With lithium aluminium tetrahydride; silica gel; In diethyl ether; acetonitrile;
DOI:10.1039/b303790h