2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate

Base Information

• Chemical Name: 2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate
• CAS No.: 245732-46-1
• Molecular Formula: C₁₃H₁₉NO₂S₂
• Molecular Weight: 285.431
• Mol file: 245732-46-1.mol

Synonyms:2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate

Chemical Property of 2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate

There total 5 articles about 2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methoxy-4-(2-nitro-vinyl)-benzene (3179-10-0) → 2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate (245732-46-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 90 percent / methanol

2: 76 percent / lithium aluminium hydride

3: Et₃N / CHCl₃ / 2 h

4: 1.1 g / K₂CO₃ / acetone / 1 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In methanol; chloroform; acetone;

DOI:10.1021/ol9907421

Reference yield:

1-methoxy-4-(1-methoxy-2-nitro-ethyl)-benzene (31367-41-6) → 2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate (245732-46-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 76 percent / lithium aluminium hydride

2: Et₃N / CHCl₃ / 2 h

3: 1.1 g / K₂CO₃ / acetone / 1 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In chloroform; acetone;

DOI:10.1021/ol9907421

Reference yield:

2-(p-methoxyphenyl)-2-methoxyethylamine (31367-42-7) → 2-(p-methoxyphenyl)-2-methoxyethyldithiocarbamate (245732-46-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CHCl₃ / 2 h

2: 1.1 g / K₂CO₃ / acetone / 1 h / Heating

With potassium carbonate; triethylamine; In chloroform; acetone;

DOI:10.1021/ol9907421

upstream raw materials:

methyl iodide

1-methoxy-4-(2-nitro-vinyl)-benzene

1-methoxy-4-(1-methoxy-2-nitro-ethyl)-benzene

2-(p-methoxyphenyl)-2-methoxyethylamine