2,4-Diacetoxybenzamide

Base Information

Chemical Name:2,4-Diacetoxybenzamide
CAS No.:195723-39-8
Molecular Formula:C₁₁H₁₁NO₅
Molecular Weight:237.212
Hs Code.:
DSSTox Substance ID:DTXSID701310625
Nikkaji Number:J906.014F

Synonyms:2,4-Diacetoxybenzamide;2,4-Bis(acetyloxy)benzamide;DTXSID701310625;195723-39-8

Suppliers and Price of 2,4-Diacetoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-Diacetoxybenzamide

Chemical Property:

XLogP3:0.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:237.06372245
Heavy Atom Count:17
Complexity:328

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OC1=CC(=C(C=C1)C(=O)N)OC(=O)C

Technology Process of 2,4-Diacetoxybenzamide

There total 3 articles about 2,4-Diacetoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50740-12-0
2,4-diacetoxybenzoyl chloride

: 195723-39-8
2,4-diacetoxybenzamide

Guidance literature:: 2,4-diacetoxybenzoyl chloride; With ammonium hydroxide; at 5 - 25 ℃; for 2h;

With dmap; acetic anhydride;

Reference yield:

: 89-86-1
4-hydroxysalicylic acid

: 195723-39-8
2,4-diacetoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂SO₄

2.1: SOCl₂ / 3 h / Heating

3.1: aq. NH₃ / 2 h / 5 - 25 °C

3.2: Ac₂O; N,N-dimethylaminopyridine

With ammonium hydroxide; thionyl chloride; sulfuric acid;

Reference yield:

: 51-01-4
2,4-bis(acetyloxy)benzoic acid

: 195723-39-8
2,4-diacetoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: SOCl₂ / 3 h / Heating

2.1: aq. NH₃ / 2 h / 5 - 25 °C

2.2: Ac₂O; N,N-dimethylaminopyridine

With ammonium hydroxide; thionyl chloride;