(E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate

Base Information

Chemical Name:(E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate
CAS No.:1208331-92-3
Molecular Formula:C₂₃H₂₁BrN₂O₃
Molecular Weight:453.335
Hs Code.:

Synonyms:(E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate

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Chemical Property of (E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate

Chemical Property:

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Technology Process of (E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate

There total 12 articles about (E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₁₅BrN₂O₂

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 1208331-92-3
(E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate

Guidance literature:: In toluene; Reflux;
DOI:10.1016/j.bmcl.2011.04.086

Reference yield:

: C₂₁H₁₉BrN₂O₃

: 1208331-92-3
(E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / toluene / 2 h / -78 °C

2: manganese(IV) oxide / dichloromethane / 48 h / Reflux

3: toluene / Reflux

With manganese(IV) oxide; diisobutylaluminium hydride; In dichloromethane; toluene; 3: Wittig reaction;
DOI:10.1016/j.bmcl.2011.04.086

Reference yield:

: C₁₉H₁₇BrN₂O₂

: 1208331-92-3
(E)-ethyl 3-(1-(4-bromophenyl)-2-(4-carbamoyl-2-methylphenyl)-1H-pyrrol-3-yl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane / 48 h / Reflux

2: toluene / Reflux

With manganese(IV) oxide; In dichloromethane; toluene; 2: Wittig reaction;
DOI:10.1016/j.bmcl.2011.04.086