benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside
CAS No.:82827-81-4
Molecular Formula:C₂₅H₃₆N₄O₇
Molecular Weight:504.583
Hs Code.:

Synonyms:benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Suppliers and Price of benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

There total 5 articles about benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 82827-80-3
benzyl 2-acetamido-4-chloro-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-galactopyranoside

: 82827-81-4
benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 140 ℃; for 24h; Heating;
DOI:10.1016/S0008-6215(00)80689-8

Reference yield:

: 82827-77-8
Benzyl-2-acetamido-2-desoxy-3,6-di-O-dibenzoyl-α-D-glucopyranosid

: 82827-81-4
benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / triphenylphosphine / CCl₄ / 15 h / Heating

2: 83 percent / 1.) methanol; 2.) Amberlite IR-120 (H⁺) resin / 1.) sodium methoxide / 0.5 h / Ambient temperature

3: 94 percent / 1.) p-toluenesulfonic acid monohydrate; 2.) Amberlite IRA-410 (OH^-) resin / dioxane / 2 h / Ambient temperature

4: 49 percent / sodium azide / dimethylformamide / 24 h / 140 °C / Heating

With methanol; sodium azide; Amberlite IR-120 (H⁺) resin; Amberlite IRA-410 (OH^-) resin; toluene-4-sulfonic acid; triphenylphosphine; sodium methylate; In 1,4-dioxane; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80689-8

Reference yield:

: 82827-78-9
benzyl 2-acetamido-3,6-di-O-benzoyl-4-chloro-2,4-dideoxy-α-D-galactopyranoside

: 82827-81-4
benzyl 2-acetamido-4-azido-2,4-dideoxy-3,6-di-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 1.) methanol; 2.) Amberlite IR-120 (H⁺) resin / 1.) sodium methoxide / 0.5 h / Ambient temperature

2: 94 percent / 1.) p-toluenesulfonic acid monohydrate; 2.) Amberlite IRA-410 (OH^-) resin / dioxane / 2 h / Ambient temperature

3: 49 percent / sodium azide / dimethylformamide / 24 h / 140 °C / Heating

With methanol; sodium azide; Amberlite IR-120 (H⁺) resin; Amberlite IRA-410 (OH^-) resin; toluene-4-sulfonic acid; sodium methylate; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80689-8