(E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene

Base Information

• Chemical Name: (E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene
• CAS No.: 1006685-31-9
• Molecular Formula: C₃₇H₃₄O₃
• Molecular Weight: 526.675
• Mol file: 1006685-31-9.mol

Synonyms:(E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene

Chemical Property of (E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene

There total 1 articles about (E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.9%

diethyl <3,5-bis(benzyloxy)benzyl>phosphonate (33617-49-1) + 3,5-dimethyl-4-benzyloxy benzaldehyde (144896-51-5) → (E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene (1006685-31-9)

Guidance literature:

diethyl <3,5-bis(benzyloxy)benzyl>phosphonate; With sodium hydride; In tetrahydrofuran; at -8 ℃; for 0.5h;

3,5-dimethyl-4-benzyloxy benzaldehyde; In tetrahydrofuran; at 25 ℃; for 16h; Further stages.;

DOI:10.1021/tx7003008

Reference yield: 68.6%

(E)-2-(benzyloxy)-5-[3,5-bis(benzyloxy)styryl]-1,3-dimethylbenzene (1006685-31-9) → (E)-5-(4-hydroxy-3,5-dimethylstyryl)benzene-1,3-diol (1006685-24-0)

Guidance literature:

With aluminium trichloride; N,N-dimethyl-aniline; In dichloromethane; at 0 ℃; for 16h;

DOI:10.1021/tx7003008

upstream raw materials:

diethyl <3,5-bis(benzyloxy)benzyl>phosphonate

3,5-dimethyl-4-benzyloxy benzaldehyde

Downstream raw materials:

(E)-5-(4-hydroxy-3,5-dimethylstyryl)benzene-1,3-diol