benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride

Base Information

Chemical Name:benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride
CAS No.:78797-01-0
Molecular Formula:C₂₈H₂₅NO₅S*ClH
Molecular Weight:524.037
Hs Code.:

Synonyms:benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride

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Technology Process of benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride

There total 3 articles about benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 78797-00-9
3,4-di-O-benzoyl-1-cyano-2,6-dideoxy-L-arabino-hex-1-enopyranose

: 100-53-8
phenylmethanethiol

: 78797-01-0
benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 72h;
DOI:10.1021/jm00143a006

Reference yield:

: 77451-26-4
1-cyano-2,6-dideoxy-L-arabino-hex-1-enopyranose

: 78797-01-0
benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / 2 h / 60 °C

2: 92 percent / HCl gas / diethyl ether / 72 h

With pyridine; hydrogenchloride; In diethyl ether;
DOI:10.1021/jm00143a006

Reference yield:

: 98-88-4
benzoyl chloride

: 78797-01-0
benzyl (3,4-di-O-benzoyl-2,6-dideoxy-L-arabino-hex-1-enopyranosyl)thioimidate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / 2 h / 60 °C

2: 92 percent / HCl gas / diethyl ether / 72 h

With pyridine; hydrogenchloride; In diethyl ether;
DOI:10.1021/jm00143a006