methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate

Base Information

Chemical Name:methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate
CAS No.:1367074-99-4
Molecular Formula:C₂₂H₂₇NO₄
Molecular Weight:369.461
Hs Code.:

Synonyms:methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate

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Chemical Property of methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate

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Technology Process of methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate

There total 5 articles about methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1367075-11-3
C₁₈H₁₅⁽²⁾H₂NO₃

: 1367074-91-6
allyl 2-(4-methoxyphenylimino)-2-(3-methoxyphenyl)acetate

: 563-43-9
ethylaluminum dichloride

: 96-10-6
diethylaluminium chloride

: 1367075-12-4
C₂₁H₂₃⁽²⁾H₂NO₃

: 1367074-99-4
methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate

Guidance literature:: C₁₈H₁₅⁽²⁾H₂NO₃; allyl 2-(4-methoxyphenylimino)-2-(3-methoxyphenyl)acetate; ethylaluminum dichloride; diethylaluminium chloride; In 1,2-dimethoxyethane; hexane; at 40 ℃; for 6.5h; Inert atmosphere;

With water; Rochelle's salt; In 1,2-dimethoxyethane; hexane; at 20 ℃; for 0.5h;

diazomethane; In diethyl ether; at 0 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2012.01.133

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: C₂₁H₂₅NO₄

: 1367074-99-4
methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate

Guidance literature:: In diethyl ether; at 0 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2012.01.133

Reference yield:

: 1367075-18-0
allyl 2-(3-methoxyphenyl)-2-oxoacetate

: 1367074-99-4
methyl 2-[N-ethyl-N-(4-methoxyphenyl)amino]-2-(3-methoxyphenyl)pent-4-enoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / benzene / 22 h / Inert atmosphere; Reflux

2.1: 1,2-dimethoxyethane; hexane / 6.5 h / 40 °C / Inert atmosphere

2.2: 0.5 h / 20 °C

2.3: 0.17 h / 0 °C

With toluene-4-sulfonic acid; In 1,2-dimethoxyethane; hexane; benzene;
DOI:10.1016/j.tetlet.2012.01.133