C₅H₁₀NCH₂C₆H₃(ONH₂)O⁽¹⁵⁾NH₂

Base Information

• Chemical Name: C₅H₁₀NCH₂C₆H₃(ONH₂)O⁽¹⁵⁾NH₂
• CAS No.: 269727-00-6
• Molecular Formula: C₁₂H₁₉N₃O₂
• Molecular Weight: 238.295
• Mol file: 269727-00-6.mol

Synonyms:C₅H₁₀NCH₂C₆H₃(ONH₂)O⁽¹⁵⁾NH₂

Chemical Property of C₅H₁₀NCH₂C₆H₃(ONH₂)O⁽¹⁵⁾NH₂

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of C₅H₁₀NCH₂C₆H₃(ONH₂)O⁽¹⁵⁾NH₂

There total 1 articles about C₅H₁₀NCH₂C₆H₃(ONH₂)O⁽¹⁵⁾NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

C30H31N2(15)NO6 → C5H10NCH2C6H3(ONH2)O(15)NH2 (269727-00-6)

Guidance literature:

With hydrazine hydrate; In methanol; chloroform;

DOI:10.1021/ja993844v

Reference yield:

(HO)2BC6H4C(2)HO + (HO)2(10)BC6H4CHO (269727-10-8) + (HO)2BC6(2)H4C(2)HO + trifluoroacetic acid (76-05-1) + C5H10NCH2C6H3(ONH2)O(15)NH2 (269727-00-6) → C5H10NHCH2C6H3(ONCHC6H4(10)B(OH)2)O(15)NC(2)HC6(2)H4B(OH)2(1+) + C5H10NHCH2C6H3(ONC(2)HC6H4B(OH)2)O(15)NCHC6H4(10)B(OH)2(1+) + C5H10NHCH2C6H3(ONCHC6H4(10)B(OH)2)O(15)NC(2)HC6H4B(OH)2(1+) + C5H10NHCH2C6H3(ONC(2)HC6H4B(OH)2)O(15)NC(2)HC6H4B(OH)2(1+) + C5H10NHCH2C6H3(ONCHC6H4(10)B(OH)2)O(15)NCHC6H4(10)B(OH)2(1+)

Guidance literature:

In dimethyl sulfoxide; solns. of formylboronic acids in DMSO mixed in equal vols.; 1% CF3CO2H added; added to aminooxy compd. soln. (stoichiometry: 1.25 equiv. of formylboronic acid per aminooxy group); 24 h; further products; without isolation; detd. by mass spectrometry;

DOI:10.1021/ja993844v

Reference yield:

(HO)2BC6H4C(2)HO + (HO)2(10)BC6H4CHO (269727-10-8) + (HO)2BC6(2)H4C(2)HO + trifluoroacetic acid (76-05-1) + C5H10NCH2C6H3(ONH2)O(15)NH2 (269727-00-6) → C5H10NHCH2C6H3(ONC(2)HC6(2)H4B(OH)2)O(15)NC(2)HC6H4B(OH)2(1+) + C5H10NHCH2C6H3(ONC(2)HC6H4B(OH)2)O(15)NC(2)HC6(2)H4B(OH)2(1+) + C5H10NHCH2C6H3(ONC(2)HC6(2)H4B(OH)2)O(15)NC(2)HC6(2)H4B(OH)2(1+) + C5H10NHCH2C6H3(ONCHC6H4(10)B(OH)2)O(15)NCHC6H4(10)B(OH)2(1+) + C5H10NHCH2C6H3(ONC(2)HC6(2)H4B(OH)2)O(15)NCHC6H4(10)B(OH)2(1+)

Guidance literature:

In dimethyl sulfoxide; solns. of formylboronic acids in DMSO mixed in equal vols.; 1% CF3CO2H added; added to aminooxy compd. soln. (stoichiometry: 1.25 equiv. of formylboronic acid per aminooxy group); 24 h; further products; without isolation; detd. by mass spectrometry;

DOI:10.1021/ja993844v