1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene

Base Information

• Chemical Name: 1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene
• CAS No.: 1114569-79-7
• Molecular Formula: C₄₇H₆₂BrNO₆
• Molecular Weight: 816.916

Synonyms:1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene

Chemical Property of 1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene

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Technology Process of 1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene

There total 1 articles about 1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

2-[3-[3-(5-tert-butyl-3-nitrosalicyl)-5-tert-butylsalicyl]-5-tert-butylsalicyl]-6-bromo-4-tert-butylphenol (1114569-76-4) + methyl iodide (74-88-4) → 1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene (1114569-79-7)

Guidance literature:

With caesium carbonate; In acetone; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1021/ol8028912

Reference yield: 91.0%

1-[3-[3-(5-tert-butyl-2-methoxy-3-nitrobenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-bromo-5-tert-butyl-2-methoxybenzene (1114569-79-7) → 1-[3-[3-(3-bromo-5-tert-butyl-2-methoxybenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-amino-5-tert-butyl-2-methoxybenzene (1114569-81-1)

Guidance literature:

With acetic acid; zinc; In ethanol; for 1h; Inert atmosphere;

DOI:10.1021/ol8028912

upstream raw materials:

2-[3-[3-(5-tert-butyl-3-nitrosalicyl)-5-tert-butylsalicyl]-5-tert-butylsalicyl]-6-bromo-4-tert-butylphenol

methyl iodide

Downstream raw materials:

1-[3-[3-(3-bromo-5-tert-butyl-2-methoxybenzyl)-5-tert-butyl-2-methoxybenzyl]-5-tert-butyl-2-methoxybenzyl]-3-amino-5-tert-butyl-2-methoxybenzene

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