ba-D-Glucopyranosiduronic acid, methyl 4-O-methyl- (9CI)

Base Information

Chemical Name:ba-D-Glucopyranosiduronic acid, methyl 4-O-methyl- (9CI)
CAS No.:762229-10-7
Molecular Formula:C₈H₁₄O₇
Molecular Weight:222.195
Hs Code.:
Mol file:762229-10-7.mol

Synonyms:bta-D-Glucopyranosiduronicacid,methyl4-O-methyl-(9CI);ba-D-Glucopyranosiduronic acid, methyl 4-O-methyl- (9CI)

Suppliers and Price of ba-D-Glucopyranosiduronic acid, methyl 4-O-methyl- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ba-D-Glucopyranosiduronic acid, methyl 4-O-methyl- (9CI)

Chemical Property:

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Technology Process of ba-D-Glucopyranosiduronic acid, methyl 4-O-methyl- (9CI)

There total 4 articles about ba-D-Glucopyranosiduronic acid, methyl 4-O-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 27551-99-1
methyl 4-O-methyl-α-D-glucopyranoside

: 73703-00-1,762229-10-7
methyl 4-O-methyl-α-D-glucopyranosiduronic acid

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium bromide; In water; at 0 ℃; for 1h; pH from 10 to 11;
DOI:10.1016/0008-6215(95)00087-A

Reference yield:

: 321907-90-8
3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

: 73703-00-1,762229-10-7
methyl 4-O-methyl-α-D-glucopyranosiduronic acid

: 5406-18-8
3-(p-methoxyphenyl)-1-propanol

Guidance literature:: With hydrogenchloride; In acetonitrile; at 20 ℃; Kinetics;
DOI:10.1135/cccc20001609

Reference yield:

: 57784-06-2,6344-46-3
methyl 2,3,6-tri-O-benzoyl-α-D-glucopyranoside

: 73703-00-1,762229-10-7
methyl 4-O-methyl-α-D-glucopyranosiduronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 72 h

2: 100 percent / NaOCH₃ / methanol / Ambient temperature

3: 90 percent / TEMPO, NaBr, sodium hypochlorite / H₂O / 1 h / 0 °C / pH from 10 to 11

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; 2,6-di-tert-butyl-4-methylpyridine; sodium methylate; sodium bromide; In methanol; dichloromethane; water;
DOI:10.1016/0008-6215(95)00087-A