C₁₄H₁₈BrNO₂

Base Information

• Chemical Name: C₁₄H₁₈BrNO₂
• CAS No.: 1242077-82-2
• Molecular Formula: C₁₄H₁₈BrNO₂
• Molecular Weight: 312.206
• Mol file: 1242077-82-2.mol

Synonyms:C₁₄H₁₈BrNO₂

Chemical Property of C₁₄H₁₈BrNO₂

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of C₁₄H₁₈BrNO₂

There total 1 articles about C₁₄H₁₈BrNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

C13H16BrNO2 (1242077-77-5) + methyl iodide (74-88-4) → C14H18BrNO2 (1242077-82-2)

Guidance literature:

C₁₃H₁₆BrNO₂; With sodium hydride; In tetrahydrofuran; mineral oil; for 1h; Inert atmosphere; Cooling;

methyl iodide; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo101401z

Reference yield: 80.0%

C14H18BrNO2 (1242077-82-2) → C14H19NO2 (1242077-91-3) + C14H17NO2 (1242077-87-7)

Guidance literature:

With sodium t-butanolate; In 1,4-dioxane; at 55 ℃; for 96h; Inert atmosphere;

DOI:10.1021/jo101401z

upstream raw materials:

C₁₃H₁₆BrNO₂

methyl iodide

Downstream raw materials:

C₁₄H₁₉NO₂

C₁₄H₁₇NO₂