N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine

Base Information

Chemical Name:N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine
CAS No.:476310-35-7
Molecular Formula:C₁₉H₃₁NO₂Si
Molecular Weight:333.546
Hs Code.:

Synonyms:N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine

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Chemical Property of N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine

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Technology Process of N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine

There total 3 articles about N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 53215-95-5
N-(trimethylsilylmethyl)benzylamine

: 133814-94-5
(2S,3R)-2,3-O-isopropylidene-1-O-p-tosyl-4-pentene-1,2,3-triol

: 476310-35-7
N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In acetonitrile; for 72h; Heating;
DOI:10.1039/b307455b

Reference yield:

: 114817-96-8
[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methanol

: 476310-35-7
N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

2: 58 percent / Cs₂CO₃; tetra-n-butylammonium iodide / acetonitrile / 72 h / Heating

With pyridine; tetra-(n-butyl)ammonium iodide; caesium carbonate; In dichloromethane; acetonitrile;
DOI:10.1039/b307455b

Reference yield:

: 188567-96-6
(3R,4R)-5-(tert-butyldimethylsiloxy)-3,4-(isopropylidenedioxy)pent-1-ene

: 476310-35-7
N-benzyl-N-[(trimethylsilyl)methyl]-N-{[(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methyl}amine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / TBAF / tetrahydrofuran / 4 h / 20 °C

2: 95 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

3: 58 percent / Cs₂CO₃; tetra-n-butylammonium iodide / acetonitrile / 72 h / Heating

With pyridine; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; caesium carbonate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1039/b307455b