N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide

Base Information

Chemical Name:N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide
CAS No.:1454909-02-4
Molecular Formula:C₃₂H₂₂Cl₂NOP
Molecular Weight:538.413
Hs Code.:

Synonyms:N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide

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Technology Process of N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide

There total 4 articles about N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 5216-30-8
1,2-bis(3-chlorophenyl)ethyne

: 6190-28-9
N,P,P-triphenylphosphinic amide

: 1454909-02-4
N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide

Guidance literature:: With potassium dihydrogenphosphate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate; In tert-butyl alcohol; for 30h;

Reference yield:

: 65887-65-2
ethyl bis(thiophen-2-yl)phosphinate

: 6190-28-9
N,P,P-triphenylphosphinic amide

: 1454909-02-4
N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide

Guidance literature:: With potassium dihydrogenphosphate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; silver carbonate; In tert-butyl alcohol; at 110 ℃; for 16h;
DOI:10.1039/c3cc44995e

Reference yield:

: 62-53-3
aniline

: 1454909-02-4
N-phenyl-3,4-di(m-chlorophenyl)-1-phenyl-1,2-dihydrobenz[c-1,2]azaphosphinine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 1 h / 50 °C

2: silver carbonate; potassium dihydrogenphosphate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen / tert-butyl alcohol / 16 h / 110 °C

With potassium dihydrogenphosphate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; silver carbonate; In acetonitrile; tert-butyl alcohol;
DOI:10.1039/c3cc44995e