2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate

Base Information

• Chemical Name: 2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate
• CAS No.: 1207471-71-3
• Molecular Formula: C₂₅H₂₀ClF₆N₃O₅S
• Molecular Weight: 623.96

Synonyms:2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate

Chemical Property of 2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate

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Technology Process of 2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate

There total 1 articles about 2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-chloro-N-(3-{[4-(1,1,1,3,3,3-hexafluoro-2-hydroxy-propan-2-yl)-2,6-dimethylphenyl]carbamoyl } phenyl)pyridine-3-carboxamide (1207471-70-2) + methanesulfonyl chloride (124-63-0) → 2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate (1207471-71-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

Reference yield: 70.0%

2-(4-{[(3-{[(2-chloropyridin-3-yl)carbonyl]amino}phenyl)carbonyl]amino}-3,5-dimethylphenyl)-1,1,1,3,3,3-hexafluoroprop-2-yl methanesulfonate (1207471-71-3) + 3-bromo-1H-pyrazole (14521-80-3,1174132-74-1) → N-[3-({4-[2-(3-bromo-1H-pyrazol-1-yl)-1,1,1,3,3,3-hexafluoropropan-2-yl]-2,6-dimethylphenyl}carbamoyl)phenyl]-2-chloropyridine-3-carboxamide (1207466-69-0)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 4h; Cooling with ice;

upstream raw materials:

2-chloro-N-(3-{[4-(1,1,1,3,3,3-hexafluoro-2-hydroxy-propan-2-yl)-2,6-dimethylphenyl]carbamoyl } phenyl)pyridine-3-carboxamide

methanesulfonyl chloride

Downstream raw materials:

N-[3-({4-[2-(3-bromo-1H-pyrazol-1-yl)-1,1,1,3,3,3-hexafluoropropan-2-yl]-2,6-dimethylphenyl}carbamoyl)phenyl]-2-chloropyridine-3-carboxamide

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