1 8 15 22-TETRAKIS(PHENYLTHIO)-29H 31H-&

Base Information

• Chemical Name: 1 8 15 22-TETRAKIS(PHENYLTHIO)-29H 31H-&
• CAS No.: 77492-98-9
• Molecular Formula: C56H34 N8 S4
• Molecular Weight: 947.204
• Mol file: 77492-98-9.mol

Synonyms:1 8 15 22-TETRAKIS(PHENYLTHIO)-29H 31H-&;1,8,15,22-tetrakis(phenylthio)-29H,31H-phthalocya;1,8,15,22-TETRAKIS(PHENYLTHIO)-29H,*31H- PHTHALOCYAN

Chemical Property of 1 8 15 22-TETRAKIS(PHENYLTHIO)-29H 31H-&

Chemical Property:

• Melting Point: >300 °C(lit.)
• PSA: 203.18000
• LogP: 11.20230

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1 8 15 22-TETRAKIS(PHENYLTHIO)-29H 31H-&

There total 4 articles about 1 8 15 22-TETRAKIS(PHENYLTHIO)-29H 31H-& which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

3-(phenylthio)-phthalonitrile (51762-68-6) → tetra-3-(phenylthio)phthalocyanine (77492-98-9)

Guidance literature:

With sodium isopentoxide; In i-Amyl alcohol; Heating;

Reference yield:

sodium thiophenolate (930-69-8) → tetra-3-(phenylthio)phthalocyanine (77492-98-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / dimethylformamide

2: 25 percent / sodium isopentyloxide / 3-methyl-butan-1-ol / Heating

With sodium isopentoxide; In i-Amyl alcohol; N,N-dimethyl-formamide;

Reference yield:

4-Nitrophthalonitrile (31643-49-9) → tetra-3-(phenylthio)phthalocyanine (77492-98-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / dimethylformamide

2: 25 percent / sodium isopentyloxide / 3-methyl-butan-1-ol / Heating

With sodium isopentoxide; In i-Amyl alcohol; N,N-dimethyl-formamide;

upstream raw materials:

3-(phenylthio)-phthalonitrile

4-Nitrophthalonitrile

3-nitrobenzene-1,2-dicarbonitrile

sodium thiophenolate

Refernces