methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside

Base Information

Chemical Name:methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside
CAS No.:688800-00-2
Molecular Formula:C₃₅H₄₈O₇Si
Molecular Weight:608.847
Hs Code.:

Synonyms:methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside

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Chemical Property of methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside

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Technology Process of methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside

There total 3 articles about methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2746-25-0
p-Methoxybenzyl bromide

: 688799-98-6
methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-D-mannopyranoside

: 688800-00-2
methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 4h;
DOI:10.1016/j.tet.2004.02.017

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 688800-00-2
methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / imidazole / CH₂Cl₂ / 1 h

2: 73 percent / NaH / tetrahydrofuran / 4 h

With 1H-imidazole; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2004.02.017

Reference yield:

: 57783-73-0,79218-74-9,81561-89-9,86172-90-9,79218-87-4
methyl 3,4-di-O-benzyl-α-D-mannopyranoside

: 688800-00-2
methyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-2-O-(p-methoxybenzyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / imidazole / CH₂Cl₂ / 1 h

2: 73 percent / NaH / tetrahydrofuran / 4 h

With 1H-imidazole; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2004.02.017