C₃₇H₆₀N₆O₉Si

Base Information

Chemical Name:C₃₇H₆₀N₆O₉Si
CAS No.:1426657-05-7
Molecular Formula:C₃₇H₆₀N₆O₉Si
Molecular Weight:761.004
Hs Code.:

C<sub>37</sub>H<sub>60</sub>N<sub>6</sub>O<sub>9</sub>Si

Synonyms:C₃₇H₆₀N₆O₉Si

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Chemical Property of C₃₇H₆₀N₆O₉Si

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Technology Process of C₃₇H₆₀N₆O₉Si

There total 20 articles about C₃₇H₆₀N₆O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₅₄N₄O₈Si

: 29883-25-8,673485-72-8
(S)-3-aminopiperidine-2,6-dione

: 1426657-05-7
C₃₇H₆₀N₆O₉Si

Guidance literature:: With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3cc00178d

Reference yield:

: 1426657-17-1
C₂₈H₄₇N₃O₇Si

: 1426657-05-7
C₃₇H₆₀N₆O₉Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium periodate; rhodium(III) chloride hydrate / acetonitrile; water; acetone / 2 h / 20 - 25 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / Inert atmosphere

3.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere

3.2: 2 h / -20 °C / Inert atmosphere

4.1: lithium hydroxide; water / methanol; tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

5.1: 4-methyl-morpholine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; 1-hydroxy-7-aza-benzotriazole / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; sodium periodate; 1-hydroxy-7-aza-benzotriazole; rhodium(III) chloride hydrate; palladium 10% on activated carbon; water; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; lithium hydroxide; isobutyl chloroformate; In tetrahydrofuran; methanol; water; acetone; acetonitrile;
DOI:10.1039/c3cc00178d

Reference yield:

: 1426656-67-8
C₃₄H₆₁N₃O₇Si₂

: 1426657-05-7
C₃₇H₆₀N₆O₉Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: (1S)-10-camphorsulfonic acid / dichloromethane; methanol / 2 h / 0 - 20 °C / Inert atmosphere

2.1: sodium periodate; rhodium(III) chloride hydrate / acetonitrile; water; acetone / 2 h / 20 - 25 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / Inert atmosphere

4.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere

4.2: 2 h / -20 °C / Inert atmosphere

5.1: lithium hydroxide; water / methanol; tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

6.1: 4-methyl-morpholine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; 1-hydroxy-7-aza-benzotriazole / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; sodium periodate; 1-hydroxy-7-aza-benzotriazole; rhodium(III) chloride hydrate; palladium 10% on activated carbon; (1S)-10-camphorsulfonic acid; water; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; lithium hydroxide; isobutyl chloroformate; In tetrahydrofuran; methanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1039/c3cc00178d