benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

Base Information

Chemical Name:benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate
CAS No.:1259283-05-0
Molecular Formula:C₂₆H₃₂N₂O₆
Molecular Weight:468.55
Hs Code.:

Synonyms:benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

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Chemical Property of benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

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Technology Process of benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

There total 1 articles about benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 59830-60-3
benzyl (1S)-(1-formyl-2-phenylethyl)carbamate

: 77877-19-1,165657-81-8
N-isopropyl oxazolidinone

: 1259283-05-0
benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

Guidance literature:: N-isopropyl oxazolidinone; With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 4 ℃; for 0.75h;

benzyl (1S)-(1-formyl-2-phenylethyl)carbamate; In dichloromethane; at -78 - 20 ℃; for 17h;
DOI:10.1002/chem.201000963

Reference yield: 95.0%

: 1259283-05-0
benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 1259283-06-1
O-(2S,3S,4S)-1-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-2-methyl-1-oxo-5-phenyl-4-(benzyloxycarbonyl)aminopentan-3-yl 1H-imidazole-1-carbothioate

Guidance literature:: In tetrahydrofuran; for 18h; Reflux;
DOI:10.1002/chem.201000963

Reference yield:

: 1259283-05-0
benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

: 1426657-10-4
C₂₀H₂₃NO₅

Guidance literature:: With water; dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3cc00178d