5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide

Base Information

Chemical Name:5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide
CAS No.:24958-43-8
Molecular Formula:C₃₁H₃₀BrNO₄
Molecular Weight:560.487
Hs Code.:

Synonyms:5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide

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Technology Process of 5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide

There total 5 articles about 5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid

: 38961-21-6
[2-(4-benzyloxy-phenyl)-ethyl]methylamine

: 24958-43-8
5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide

Guidance literature:: With phenylboronic acid; In toluene; at 110 ℃; for 30h;
DOI:10.1080/00397910802029067

Reference yield: 83.0%

: 38961-21-6
[2-(4-benzyloxy-phenyl)-ethyl]methylamine

: 27240-64-8
5-Benzyloxy-2-bromo-4-methoxybenzoylchlorid

: 24958-43-8
5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide

Guidance literature:: With sodium hydroxide; In chloroform; water; at 20 ℃;

Reference yield:

: 873195-14-3
5-benzyloxy-2-bromo-4-methoxy benzoic acid benzotriazole-1-yl ester

: 38961-21-6
[2-(4-benzyloxy-phenyl)-ethyl]methylamine

: 24958-43-8
5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide

Guidance literature:: 5-benzyloxy-2-bromo-4-methoxy benzoic acid benzotriazole-1-yl ester; [2-(4-benzyloxy-phenyl)-ethyl]methylamine; With potassium carbonate; In chloroform; at 25 - 30 ℃; for 0.5 - 1.5h;

With sodium hydroxide; In methanol; at 0 - 30 ℃; for 1.5 - 3h; Product distribution / selectivity;