DANSYL-DL-NORVALINE PIPERIDINIUM SALT

Base Information

• Chemical Name: DANSYL-DL-NORVALINE PIPERIDINIUM SALT
• CAS No.: 77426-57-4
• Molecular Formula: C₁₇H₂₂N₂O₄S
• Molecular Weight: 350.439
• Hs Code.: 2935009090
• Mol file: 77426-57-4.mol

Synonyms:DL-Norvaline,N-[[5-(dimethylamino)-1-naphthalenyl]sulfonyl]-; DL-Dansylnorvaline;Dansyl-DL-norvaline; N-Dansyl-DL-norvaline

Chemical Property of DANSYL-DL-NORVALINE PIPERIDINIUM SALT

Chemical Property:

• Vapor Pressure: 1.4E-12mmHg at 25°C
• Refractive Index: 1.609
• Boiling Point: 542°C at 760 mmHg
• Flash Point: 281.6°C
• PSA: 95.09000
• Density: 1.282g/cm³
• LogP: 3.90910
• Storage Temp.: −20°C

Purity/Quality:

98% ^*data from raw suppliers

DANSYL-DL-NORVALINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DANSYL-DL-NORVALINE PIPERIDINIUM SALT

There total 1 articles about DANSYL-DL-NORVALINE PIPERIDINIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-aminopentanoic acid (760-78-1,498-18-0) + 5-(dimethylamino)naphth-1-ylsulfonyl chloride (605-65-2) → dansyl norvaline (77426-57-4,77426-55-2)

Guidance literature:

In acetone;

DOI:10.1021/ja00268a040

Reference yield:

dansyl norvaline (77426-57-4,77426-55-2) → 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-pentanoic acid + 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-pentanoic acid

Guidance literature:

With phosphate buffer; sodium dodecyl-sulfate; vancomycin; at 20 ℃; Product distribution; electrophoretic enantioseparations, various substrates;

DOI:10.1021/ac00109a030

upstream raw materials:

2-aminopentanoic acid

5-(dimethylamino)naphth-1-ylsulfonyl chloride

Refernces